ANALISA KADAR LOGAM TIMBAL DAN BESI PADA SUSU KENTAL MANIS KEMASAN KALENG YANG BEREDAR DI KELURAHAN TANJUNG SARI DENGAN METODE SPEKTROFOTOMETRI SERAPAN ATOM (SSA)
Keywords:
Lead, Iron, Sweetened Condensed Milk, Atomic Absorption SpectrophotometryAbstract
Sweetened condensed milk is cow's milk in which the water is removed and added sugar, resulting in milk that is very sweet in taste and can last for a year if it is not opened. Sweetened condensed milk products, powdered milk, and sterile milk are often made in packaging made of plastic and cans to avoid the influence of sunlight, packaging time, storage and others. And as a result of the packaging, the product is often damaged either microbiologically, mechanically or chemically. These cans are lined with other coating materials with certain protection. This is to prevent a reaction that could cause the can to corrode and leak. The presence of these metals, even in small levels, will endanger the health of consumers and considering that heavy metals will accumulate in the body, so that gradually the levels will increase and are very dangerous to health, including Pb and Fe metals that can act on the can. Qualitative testing is to determine the presence of the metal present in the sample and quantitative testing is to determine how much content is present in the sample. Before carrying out quantitative testing, the samples were first destroyed using wet destruction. From the results of qualitative testing, all samples contained Pb and Fe metals. From the results of quantitative testing on Pb, the lowest sample was found in sample 3 of 0.0105 mg/kg and sample 5 of 0.0105 mg/kg, this did not exceed the SNI 297.2011 threshold of 0.02 mg/kg. While the results for heavy metal Pb at large concentrations in sample 1 were 0.0239 mg/kg; sample 2 of 0.0371 mg/kg, and sample of 0.0262 mg/kg exceeds the threshold of SNI 297.2011 of 0.02 mg/kg while for heavy metal Fe is still below the threshold allowed by SNI 297.2011 which is 10.0 mg/kg, namely sample 1 of 0.0081 mg/kg; sample 2 of 0.0100 mg/kg; sample 3 of 0.0079 mg/kg; sample 4 is 0.0068 mg/kg and sample 5 is 0.0122 mg/kg.
Downloads
References
Adhani R dan Kholishotunnisa S (Eds). Logam Berat Sekitar Manusia (2017). Lambung.
Andrizal dan Musanif J (Eds). Susu. Direktur Pengembangan Usaha Dan Investasi (2013). Tersedia Direktorat Pengembangan Usaha Dan Investasi.
Apridamayanti dkk Analisis Logam Timbal dalam Eye-Liner Pencil yang Beredar di Kota Pontianak (2015) visual Post: Jurnal Cerebellum. 1(1):11-21
Aprilia D, Dkk. Spektrofotometer Serapan Atom Institut Ilmu Kesehatan Bhakti Wiyata Kediri (2015).
Aziz, T Pengaruh Jumlah Cacing Lumbricus Rubellus Dan Lama Waktu Remidiasi Terhadap Kandungan Logam Timbal Pada Tanah Tpa Supit Urang Malang Sebagai Sumber Belajar Biologi (Disertai Doktoral, University Of Muhammadiyah Malang, 2017).
Codex Alimentarius International Food Standards Standard For Sweetened Condensed Milks Cxs 282-1971 Adopted In 1971. Revised In 1999. Amended In 2010, 2018.
Djamilah Arifiyana Dan Ma. Hanny Ferry Fernanda Analisis Kualitatif dan Kuantitatif Cemaran Logam Berat Timbal (Pb) Dan Kadmium (Cd) Pada Produk Kosmetik Pensil Alis Menggunakanspektrofotometer Serapan Atom (SSA) (2018) 4(1): Juni 2460 – 5972
Djunaidi C Studi Interfensi Pada AAS Fakultas Sains Dan Matematika Semarang (2018).
Fiskanita, Dkk.Analisis Logam Timbal (Pb) Dan Besi (Fe) Dalam Air Laut Di Wilayah Pesisir Pelabuhan Ferry Taipa Kecamatan Palu Utara (2012).1(4): 181-186, 2302-6030.
Farida S. “susu kental manis dan krimmer kental manis”. Tersedia di Food review Indonesia (2012). 7 (7): 22-25
Godam.2012. Isi Kandungan Gizi Biji Nangka - Komposisi Nutrisi Bahan Makanan.(online).Tersedia: http://www.organisasi.org/1970/01/isikandungan-gizi-biji-nangka-komposisi-nutrisi-bahan-makanan.html (diakses pada selasa, 1 maret 2022).
Harurani, L. (2011) Analisa kandungan logam berat Pb dan Fe dengan metode spektrofotometri serapan atom terhadap susu kental manis di pekanbaru. Fakultas Tarbiyah dan Keguruan Universitas Islam Negri Sultan Syarif Kasim Riau Pekanbaru.
Hasrini R F dan Khoiriyah A Analisis Produk Krimer Kental Manis Dalam Rangka Pengembangan Standar Nasional Indonesia Baru (2018). Visual post : Balai Besar Industri Agro (BBIA), Kementerian Perindustrian Jl. Ir. H. Juanda No. 11, Bogor 16122.
Perdana W. analisis logam berat di kemasan kaleng (2019). 9 (2):64-66
Rasyid R, dkk. Analisis Kadmium (CD), Seng (Zn) dan Timbal (Pb) Pada Susu Kental Manis Kemasan Kaleng Secara Spektrofotometri Serapan Atom (SSA) (2013). 4 (5) 78-87
Santoso B, dkk. Dampak Kandungan Timbal (Pb) Dalam Udara Terhadap Kecerdasan Anak Sekolah Dasar (2011). 1 (2) 14-20
Saputro dkk Identifikasi Kualitatif Kandungan Logam Berat (Pb, Cd, Cu, Dan Zn) Pada Ikan Sapu-Sapu (Hypostomus Plecostomus) Di Sungai Pabelan Kartasura Tahun 2012 (2012). Visual post : 3 Pendidikan Biologi FKIP-Universitas Muhammadiyah Surakarta.
Saraswati, I. Paper, Skripsi: Analisis Arsen Pada Beras Dan Hasil Tanakannya Secara Spektrofotometri Serapan Atom .(2018). Medan Universitas Sumatera Utara
Sinurat dkk. Analisis kadar zat besi pada sari kedelai kemasan dengan metode spektrofotometri UV-VIS (2021) .3 (2)74-79.
SNI 2971:2011 Standar Nasional Indonesia Susu Kental Manis
Sudiarta I.W & Suarya,P (2019). Kadar Fe dan Zn dalam krim Kental Manis kemasan kaleng Expire dan non expire menggunakan hydrogen peroksida (H2O2) untuk destruksi basah secara spektrofotometri serapan atom (SSA). Visual post : DOI: https://doi.org/10.24843/JCHEM.2019.v13.i02.p08.
Sutrisno (2009). Teknologi Pengolahan Susu. eBookPangan.com.
Yani A (2021). Pengaruh logam berat pada kesehatan. Peneliti Ahli Madya BPTP Lampung diakses tanggal: 9 maret 2021 .
Yanti W, dkk Gambaran Kadar Timbal Dalam Darah Petugas Operator Spbu 54.801.45. (2020) Diploma thesis, Poltekkes Kemenkes Denpasar Jurusan Teknologi Laboratorium Medis.
Yerimadesi dkk. analisis kadar logam timbal (Pb) dan tembaaga (Cu) pada susu kental manis kemasan kaleng. (2012) Visual post: Chemistry journal of state university of padang
